Qualifications Summary

  • Over 27 years experience in wet chemistry, GC, and HPLC.

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  • Manages organic preparatory and wet chemistry laboratories.

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  • Waters Associates Liquid Chromatographic Maintenance School.

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  • Dupont Thermal Analysis Training.
NANCY A. ROSE
Sample Preparatory Section Head
 
Professional Affiliations

Independent Testing Laboratories Association

Fields of Expertise

Extensive working knowledge of, but not limited to, gas chromatographs, liquid chromatographs, differential scanning calorimeter, UV spectrophotometer, infared spectrophotometer, potentiographs, atomic absorption spectrophotometer, and Hewlett Packard 335B automated computer system.

Education

University of Massachusetts, Dartmouth – Chemistry Course (1988)
Computer Course – Rhode Island College (1984)

Employment History

1997-Present  Woods Hole Group
                       Environmental Laboratories

1989-1997      Inchcape Testing Services, Inc.
1988-1989      GHR Analytical
1972-1988      Ciba-Geigy Corporation
1984-1987      Cambridge Analytical Associates
Key Projects

Lake Waban Ecological Risk Assessment, Wellesley, Massachusetts.  Confidential Client.  Sample Preparation Supervisor.
Woods Hole Group provided quarterly sampling and analysis of surface water, sediment and tissues in support of an ecological risk assessment.  Surface water metals were sampled and analyzed using “clean” techniques, i.e. Class 100 clean hood conditions, according to Method 1669.  Additional water analyses included cyanide, hexavalent chromium, total suspended solids and hardness.  Sediments were analyzed for metals, physiologically available cyanide (PACN), hexavalent chromium and acid volatile sulfide/simultaneously extractable metals (AVS/SEM).  Fish tissue, mussels, clams, invertebrates and aquatic plants were analyzed for metals.  The fish species included large mouth bass, pumpkinseed sunfish and yellow perch.  Fish tissue analyses were conducted on whole body, fillets, and livers.  Various species of aquatic plants were analyzed either as stem/leaf or root samples.

Deer Island Western Shoreline Hydrocarbon Source Evaluation, Boston Harbor, Massachusetts.  Confidential Client.  Sample Preparation Supervisor.
Woods Hole Group conducted an ecological assessment of an intertidal shoreline area on Deer Island in Boston Harbor, Massachusetts.  Mussel tissue and sediment were analyzed for alkylated and priority pollutant PAHs to identify the source of hydrocarbons at the impacted site and to support a site ecological risk characterization.  In addition to sample collection, the assessment included a semi-quantitative bioassessment survey of the intertidal biota at the impacted and reference sites.  The tissue analysis required low parts-per-billion detection limits for the PAHs to satisfy risk-based data quality objectives.  Advanced fingerprinting diagnostic techniques were used to identify the source of PAHs in the sediment and tissue residues. Results of the study indicated that PAHs in impacted site bivalves contained a large petrogenic component superimposed on a pyrogenic background observed at the reference sites.  The PAH concentrations found in the sediment were determined not to be a risk to the intertidal bentic resources.

Ten Harbors Program, New England Coastal Harbors.  Confidential Client.  Project Manager.
Woods Hole Group has analyzed sediment and tissues in support of the Ten Harbors Program implemented by the U.S. Army Corps of Engineers New England District.  More than 90 sediment samples have been analyzed in seven sample delivery groups for PAH (NS&T/EMAP list), PCB congeners (NS&T/EMAP list), pesticides, metals, and TOC.  Results have been reported on a 28-day turnaround time in Level IV data packages, suitable for full data validation and with an electronic data deliverable.  As part of this program, more than 100 tissue samples (bivalves and amphipods) have been analyzed and reported for PAHs and selected metals.

South Weymouth Naval Air Station Remedial Investigations, South Weymouth, Massachusetts.  Confidential Client.  Sample Preparation Supervisor.
Risk assessment and confirmatory analyses were performed for a fuel farm and UST remediation at the Naval Air Station in South Weymouth, Massachusetts.  Analyses included TCL VOC, SVOC and Pesticide/PCB, TAL Metals and waste characterization.  In addition, MADEP Methods for VPH/EPH, lead, copper and PCB results with 72-hour turnaround time were provided.  Full Level IV, CLP-like data packages suitable for data validation were provided for most analyses.

Gloucester Harbor Monitoring Program, Gloucester, Massachusetts.  Confidential Client.  Sample Preparation Superivsor.
In support of the City of Gloucester, Massachusetts’ 301(h) Outfall Monitoring Program, Woods Hole Group Environmental Laboratories is providing low-level measurements of volatiles (Method 8260B modified), semivolatiles (Method 8270C modified), pesticides/PCBs (Methods 8081/8082 modified), phenols, metals, cyanide, grain size and TOC in marine sediments.  The project-specific detection limits were developed to permit ecological risk assessment using sediment quality guidelines.

Waste Oil CERCLA Site,New Hampshire.  Confidential Client.  Project Manager.
In support of an EPA Superfund site remedial investigation, Woods Hole Group analyzed more than 300 soil, groundwater, surface water and sediment samples.  Sediments were analyzed for ultra-trace level PAHs, pesticides, metals and acid volatile sulfide/simultaneously extractable metals (AVS/SEM).  Required analyses for the other matrices included volatile petroleum hydrocarbons (VPH), extractable petroleum hydrocarbons (EPH), TAL metals, pesticides, PCB Aroclors and TOC.  Level IV data packages were reported and validated, by a third party, along with project-specific electronic data deliverables.

Caspian Sea Ecological Baseline Study, Caspian Sea.  Confidential Client.  Sample Preparation Supervisor.
In support of an ecological baseline study for an international oil company, Woods Hole Group Environmental Laboratories analyzed marine sediments and seawater samples for petroleum hydrocarbons, polynuclear aromatic hydrocarbons (PAHs), polychlorinated biphenyls, and total phenols.  In order to provide meaningful baseline measurements, alumina cleanup and gas chromatography with flame ionization detection was employed for petroleum hydrocarbon measurements to provide reporting limits on the order of 1 mg/Kg without interference from non-petroleum hydrocarbons.  Selected samples were analyzed for PAHs by gas chromatography/mass spectrometry with selected ion monitoring.  Data will be used for comparing sediment and water column measurements from future monitoring surveys.

Publications and Presentations

Kane, P.J., T.C. Sauer, N. Laurianno, Jr., E.M. Hynes, C. Gauthier, J. Hart, N.A. Rose, and A.J. Laurila.  “Hydrocarbon Characterization of Petroleum Products & Coal Tar, EPH/VPH and Beyond.”  Poster Presentation at 14th Annual Conference on Contaminated Soils, Amherst, Massachusetts, 1998. 


 
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For more information please call or e-mail the
General Manager:
Nicholas P. Corso at (508) 822-9300
ncorso@whgrp.com

 
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Marine Environmental Solutions
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